2-溴-5-甲氧基苯甲腈合成路线 (共 13 条)
反应条件
1.1: thionyl chloride / 3 h / Reflux; Inert atmosphere 1.2: 16 h / 20 °C 2.1: thionyl chloride / 3 h / Reflux; Inert atmosphere View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 7 p. 2233 - 2239
反应条件
potassium hydroxide; diethylene glycol
参考文献
Frank; Fanta; Tarbell
Journal of the American Chemical Society, 1948 , vol. 70, p. 2314,2317
反应条件
1: With borane-THF in tetrahydrofuran
T=20°C; Cooling with ice;
2: With water; sodium carbonate in tetrahydrofuran
参考文献
INCYTE CORPORATION
Patent: US2010/190804 A1, 2010 ;
Location in patent: Page/Page column 75-76 ;
US 20100190804 A1