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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
13871-59-5
合成路线
（共 13 条）
56633-08-0
→
反应条件
13871-59-5
反应条件
palladium 10 on activated carbon; hydrogen in methanol T=20°C; P=760.051 Torr; 24 h;
参考文献
Crestey, Francois; Jensen, Anders A.; Borch, Morten; Andreasen, Jesper Tobias; Andersen, Jacob; Balle, Thomas; Kristensen, Jesper Langgaard
Journal of Medicinal Chemistry, 2013 , vol. 56, # 23 p. 9673 - 9682
120493-95-0
→
反应条件
13871-59-5
反应条件
toluene-4-sulfonic acid; palladium on activated charcoal in methanol; water 24 h; Heating;
参考文献
Hara; Akiba; Miyashita; Hoshino; Umezawa
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 9 p. 3638 - 3641
120494-01-1
→
反应条件
13871-59-5
反应条件
hydrogen bromide; acetic acid T=80°C; 3 h;
参考文献
Hara; Akiba; Miyashita; Hoshino; Umezawa
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 9 p. 3638 - 3641
120493-94-9
→
反应条件
13871-59-5
反应条件
1: 47 percent / diethyl ether; methanol / 72 h / Ambient temperature 2: 22 percent / p-TsOH*H2O / 10percent Pd/C / methanol; H2O / 24 h / Heating View Scheme
参考文献
Hara; Akiba; Miyashita; Hoshino; Umezawa
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 9 p. 3638 - 3641
34882-51-4
→
反应条件
13871-59-5
反应条件
1: 88 percent / NaBH4 / methanol / 2 h / Ambient temperature 2: 47 percent / diethyl ether; methanol / 72 h / Ambient temperature 3: 22 percent / p-TsOH*H2O / 10percent Pd/C / methanol; H2O / 24 h / Heating View Scheme
参考文献
Hara; Akiba; Miyashita; Hoshino; Umezawa
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 9 p. 3638 - 3641
35167-81-8
3,4-二甲氧基苯乙基异氰酸酯
→
反应条件
13871-59-5
反应条件
1: 1) phosphoryl chloride / 1) reflux, 1 h; 2) methylene chloride, 0 deg C, overnight 2: 75 percent / sodium hydride / benzene 3: 5 percent / methionine; methanesulphonic acid / neat (no solvent) 4: lithium aluminium hydride / tetrahydrofuran View Scheme
参考文献
Irie, Hiroshi; Shiina, Ayako; Fushimi, Tamaki; Katakawa, Jun'ichi; Fujii, Nobutaka; Yajima, Haruaki
Chemistry Letters, 1980 , p. 875 - 878
75327-43-4
→
反应条件
13871-59-5
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Irie, Hiroshi; Shiina, Ayako; Fushimi, Tamaki; Katakawa, Jun'ichi; Fujii, Nobutaka; Yajima, Haruaki
Chemistry Letters, 1980 , p. 875 - 878
34882-64-9
→
反应条件
13871-59-5
反应条件
1: 54 percent / NaBH4 / methanol / 2 h / Ambient temperature 2: 64 percent / methanol; diethyl ether / 72 h / Ambient temperature 3: 50 percent / AcOH, HBr / 3 h / 80 °C View Scheme
参考文献
Hara; Akiba; Miyashita; Hoshino; Umezawa
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 9 p. 3638 - 3641
120493-96-1
→
反应条件
13871-59-5
反应条件
1: 64 percent / methanol; diethyl ether / 72 h / Ambient temperature 2: 50 percent / AcOH, HBr / 3 h / 80 °C View Scheme
参考文献
Hara; Akiba; Miyashita; Hoshino; Umezawa
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 9 p. 3638 - 3641
493-49-2
6,7-二甲氧基-3,4-二氢-异喹啉-1-酮
→
反应条件
13871-59-5
反应条件
1: 75 percent / sodium hydride / benzene 2: 5 percent / methionine; methanesulphonic acid / neat (no solvent) 3: lithium aluminium hydride / tetrahydrofuran View Scheme
参考文献
Irie, Hiroshi; Shiina, Ayako; Fushimi, Tamaki; Katakawa, Jun'ichi; Fujii, Nobutaka; Yajima, Haruaki
Chemistry Letters, 1980 , p. 875 - 878
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