2,3-二氧代-3-苯丙酸叔丁酯合成路线 （共 7 条）
反应条件
magnesium monoperoxyphthalate hexahydrate in dichloromethane; water T=20°C; 5 h;
参考文献
Lee, Kieseung; Im, Jin-Mo
Tetrahedron Letters, 2001 , vol. 42, # 8 p. 1539 - 1542
反应条件
pyridine; prehydrolyzed Dess-Martin periodinane; water in dichloromethane 4 h;
参考文献
Meyer, Stephanie D.; Schreiber, Stuart L.
Journal of Organic Chemistry, 1994 , vol. 59, # 24 p. 7549 - 7552
反应条件
1,1,1-triacetoxy-1,1-dihydro-1,2-benziodoxol-3-(1H)-one; water in dichloromethane 1.3 h;
参考文献
Meyer, Stephanie D.; Schreiber, Stuart L.
Journal of Organic Chemistry, 1994 , vol. 59, # 24 p. 7549 - 7552
反应条件
1: 1.) bis(trimethylsilyl)acetamide (BSA) / 1.) benzene, 0 deg C, 5 min, 2.) benzene, RT, 1 h 2: 69 percent / Oxone / tetrahydrofuran; H2O / 2 h / Ambient temperature View Scheme
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle K.
Tetrahedron Letters, 1991 , vol. 32, # 42 p. 6039 - 6042
反应条件
1: 1.) BSA / 1.) PhH, 10 deg C, 5 min, 2.) 25 deg C 2: Oxone, H2O / tetrahydrofuran / 2 h / Ambient temperature View Scheme
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle K.
Tetrahedron Letters, 1991 , vol. 32, # 42 p. 6039 - 6042
反应条件
1: benzene / 48 h / Heating 2: 90 percent / potassium hydroxide / H2O / 0.08 h / 0 °C 3: 1.) bis(trimethylsilyl)acetamide (BSA) / 1.) benzene, 0 deg C, 5 min, 2.) benzene, RT, 1 h 4: 69 percent / Oxone / tetrahydrofuran; H2O / 2 h / Ambient temperature View Scheme
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle; Munk, Morton E.; et al.
Heterocycles, 1993 , vol. 35, # 2 p. 975 - 995
反应条件
1: 90 percent / potassium hydroxide / H2O / 0.08 h / 0 °C 2: 1.) bis(trimethylsilyl)acetamide (BSA) / 1.) benzene, 0 deg C, 5 min, 2.) benzene, RT, 1 h 3: 69 percent / Oxone / tetrahydrofuran; H2O / 2 h / Ambient temperature View Scheme
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle; Munk, Morton E.; et al.
Heterocycles, 1993 , vol. 35, # 2 p. 975 - 995
