2,3-二氧代-3-对甲苯丙酸叔丁酯合成路线 （共 6 条）
反应条件
Oxonereg; in tetrahydrofuran; water
2 h; Ambient temperature;
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle; Munk, Morton E.; et al.
Heterocycles, 1993 , vol. 35, # 2 p. 975 - 995
反应条件
1: 96 percent / bis(trimethylsilyl)acetamide / benzene / 2 h / 25 °C
2: 91 percent / Oxone / tetrahydrofuran; H2O / 2 h / Ambient temperature
View Scheme
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle; Munk, Morton E.; et al.
Heterocycles, 1993 , vol. 35, # 2 p. 975 - 995
反应条件
1: 96 percent / bis(trimethylsilyl)acetamide / benzene / 2 h / 25 °C
2: 91 percent / Oxone / tetrahydrofuran; H2O / 2 h / Ambient temperature
View Scheme
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle; Munk, Morton E.; et al.
Heterocycles, 1993 , vol. 35, # 2 p. 975 - 995
反应条件
1: benzene / 48 h / Heating
2: 90 percent / potassium hydroxide / H2O / 0.08 h / 0 °C
3: 96 percent / bis(trimethylsilyl)acetamide / benzene / 2 h / 25 °C
4: 91 percent / Oxone / tetrahydrofuran; H2O / 2 h / Ambient temperature
View Scheme
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle; Munk, Morton E.; et al.
Heterocycles, 1993 , vol. 35, # 2 p. 975 - 995
反应条件
1: 90 percent / potassium hydroxide / H2O / 0.08 h / 0 °C
2: 96 percent / bis(trimethylsilyl)acetamide / benzene / 2 h / 25 °C
3: 91 percent / Oxone / tetrahydrofuran; H2O / 2 h / Ambient temperature
View Scheme
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle; Munk, Morton E.; et al.
Heterocycles, 1993 , vol. 35, # 2 p. 975 - 995
反应条件
1: 96 percent / oxalyl chloride, DMF / benzene / 2 h / 10 °C
2: 96 percent / bis(trimethylsilyl)acetamide / benzene / 2 h / 25 °C
3: 91 percent / Oxone / tetrahydrofuran; H2O / 2 h / Ambient temperature
View Scheme
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle; Munk, Morton E.; et al.
Heterocycles, 1993 , vol. 35, # 2 p. 975 - 995
