3-(4-甲氧基苯基)-2,3-二氧代丙酸叔丁酯合成路线 （共 6 条）
反应条件
Oxonereg; in tetrahydrofuran; water T=25°C; 2 h;
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle; Munk, Morton E.; et al.
Heterocycles, 1993 , vol. 35, # 2 p. 975 - 995
反应条件
1: 78 percent / bis(trimethylsilyl)acetamide / benzene / 2 h / 25 °C 2: 63 percent / Oxone / tetrahydrofuran; H2O / 2 h / 25 °C View Scheme
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle K.
Tetrahedron Letters, 1991 , vol. 32, # 42 p. 6039 - 6042
反应条件
1: 1.) BSA / 1.) PhH, 10 deg C , 5 min, 2.) 25 deg C 2: Oxone, H2O / tetrahydrofuran / 2 h / Ambient temperature View Scheme
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle; Munk, Morton E.; et al.
Heterocycles, 1993 , vol. 35, # 2 p. 975 - 995
反应条件
1: benzene / 48 h / Heating 2: 90 percent / potassium hydroxide / H2O / 0.08 h / 0 °C 3: 78 percent / bis(trimethylsilyl)acetamide / benzene / 2 h / 25 °C 4: 63 percent / Oxone / tetrahydrofuran; H2O / 2 h / 25 °C View Scheme
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle; Munk, Morton E.; et al.
Heterocycles, 1993 , vol. 35, # 2 p. 975 - 995
反应条件
1: 90 percent / potassium hydroxide / H2O / 0.08 h / 0 °C 2: 78 percent / bis(trimethylsilyl)acetamide / benzene / 2 h / 25 °C 3: 63 percent / Oxone / tetrahydrofuran; H2O / 2 h / 25 °C View Scheme
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle; Munk, Morton E.; et al.
Heterocycles, 1993 , vol. 35, # 2 p. 975 - 995
反应条件
1: 90 percent / oxalyl chloride, DMF / benzene / 2 h / 10 °C 2: 78 percent / bis(trimethylsilyl)acetamide / benzene / 2 h / 25 °C 3: 63 percent / Oxone / tetrahydrofuran; H2O / 2 h / 25 °C View Scheme
参考文献
Wasserman, Harry H.; Ennis, David S.; Vu, Chi B.; Schulte, Gayle; Munk, Morton E.; et al.
Heterocycles, 1993 , vol. 35, # 2 p. 975 - 995
