magnesium monoperoxyphthalate hexahydrate in dichloromethane; water T=20°C; 5 h;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '508294', constants.ctx, '0')">bis(trimethyl-silyl)acetamide</a> <br />&nbsp;1.) benzene, 0 deg C, 5 min, 2.) benzene, RT, 1 h;&nbsp;&nbsp;Yield given. Multistep reaction;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '110354', constants.ctx, '0')">4-(N,N-dimethlyamino)pyridine</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '5764110', constants.ctx, '0')">1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />&nbsp;Ambient temperature;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: benzene / 48 h / Heating<br />2: 90 percent / potassium hydroxide / H₂O / 0.08 h / 0 &deg;C<br />3: 1.) bis(trimethylsilyl)acetamide (BSA) / 1.) benzene, 0 deg C, 5 min, 2.) benzene, RT, 1 h<br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: 90 percent / potassium hydroxide / H₂O / 0.08 h / 0 &deg;C<br />2: 1.) bis(trimethylsilyl)acetamide (BSA) / 1.) benzene, 0 deg C, 5 min, 2.) benzene, RT, 1 h<br /> <br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: benzene / 48 h / Heating<br />2: 90 percent / potassium hydroxide / H₂O / 0.08 h / 0 &deg;C<br />3: 1.) bis(trimethylsilyl)acetamide (BSA) / 1.) benzene, 0 deg C, 5 min, 2.) benzene, RT, 1 h<br /> <br /> &nbsp;