N,n,N,N-四甲基-1-苯基甲烷二胺合成路线 （共 23 条）
反应条件
1: 74 percent / KOH / tetrahydrofuran / Heating
2: 68 percent / petroleum ether
View Scheme
参考文献
Nikogosyan, L. L.; Nersesyan, K. A.; Satina, T. Ya.; Panosyan, G. A.; Indzhikyan, M. G.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 4.1 p. 671 - 675
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 4 p. 749 - 754
反应条件
1: 74 percent / KOH / tetrahydrofuran / Heating
2: 68 percent / petroleum ether
View Scheme
参考文献
Nikogosyan, L. L.; Nersesyan, K. A.; Satina, T. Ya.; Panosyan, G. A.; Indzhikyan, M. G.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 4.1 p. 671 - 675
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 4 p. 749 - 754
反应条件
1: 81 percent / benzene / Heating
2: 74 percent / KOH / tetrahydrofuran / Heating
3: 68 percent / petroleum ether
View Scheme
参考文献
Nikogosyan, L. L.; Nersesyan, K. A.; Satina, T. Ya.; Panosyan, G. A.; Indzhikyan, M. G.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 4.1 p. 671 - 675
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 4 p. 749 - 754
反应条件
1: 2.) aq. NaOH / 1.) MeOH, 48 h, r.t., 2.) H2O, 0 deg C, 10 min
2: Et3N / xylene / 2 h / Ambient temperature
3: xylene / 3 h / Heating
View Scheme
参考文献
Haddad, M.; Legros, J. P.; Lopez, L.; Boisdon, M. T.; Barrans, J.
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 69, # 12 p. 189 - 196
反应条件
1: Et3N / xylene / 2 h / Ambient temperature
2: xylene / 3 h / Heating
View Scheme
参考文献
Haddad, M.; Legros, J. P.; Lopez, L.; Boisdon, M. T.; Barrans, J.
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 69, # 12 p. 189 - 196
参考文献
Hobbs,C.F.; Weingarten,H.
Journal of Organic Chemistry, 1971 , vol. 36, p. 2881 - 2885
反应条件
1: 79 percent / 3.5 h / 60 °C
2: 75 percent / petroleum ether / 4 h
View Scheme
参考文献
Nikogosyan, L. L.; Nersesyan, K. A.; Satina, T. Ya.; Panosyan, G. A.; Mirzoyan, R. G.; Indzhikyan, M. G.,
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 12.1 p. 2716 - 2721,2434 - 2438
反应条件
in xylene
3 h; Heating;
参考文献
Haddad, M.; Legros, J. P.; Lopez, L.; Boisdon, M. T.; Barrans, J.
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 69, # 12 p. 189 - 196
反应条件
in xylene
3 h; Heating;
参考文献
Haddad, M.; Legros, J. P.; Lopez, L.; Boisdon, M. T.; Barrans, J.
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 69, # 12 p. 189 - 196
反应条件
in xylene
3 h; Heating;
参考文献
Haddad, M.; Legros, J. P.; Lopez, L.; Boisdon, M. T.; Barrans, J.
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 69, # 12 p. 189 - 196
