N,N-二氯-1,1,1-三氟甲胺合成路线 (共 20 条)
反应条件
mercury(II) fluoride; bromine in monofluoro-trichloromethane
T=0°C; 96 h;
参考文献
Geisel, Martin; Waterfeld, Alfred; Mews, Ruediger
Chemische Berichte, 1985 , vol. 118, # 11 p. 4459 - 4472
反应条件
mercury(II) fluoride; bromine
参考文献
Geisel, Martin; Waterfeld, Alfred; Mews, Ruediger
Chemische Berichte, 1985 , vol. 118, # 11 p. 4459 - 4472
反应条件
mercury(II) fluoride; chlorine
T=0°C; 72 h;
参考文献
Geisel, Martin; Waterfeld, Alfred; Mews, Ruediger
Chemische Berichte, 1985 , vol. 118, # 11 p. 4459 - 4472
反应条件
mercury(II) fluoride; chlorine
T=20°C; 20 h;
参考文献
Geisel, Martin; Waterfeld, Alfred; Mews, Ruediger
Chemische Berichte, 1985 , vol. 118, # 11 p. 4459 - 4472
反应条件
chlorine
at 75°C for 1 h then 140°C for 3 h and shaking;
参考文献
Chambers,W.J. et al.
Journal of the American Chemical Society, 1962 , vol. 84, p. 2337 - 2343
反应条件
bromine; cesium fluoride
T=22°C; 12 h;
参考文献
Zheng, Yuan Y.; Bauknight, Charles W.; DesMarteau, Darryl D.
Journal of Organic Chemistry, 1984 , vol. 49, # 19 p. 3590 - 3595
反应条件
Ambient temperature;
参考文献
Geisel, Martin; Waterfeld, Alfred; Mews, Ruediger
Chemische Berichte, 1985 , vol. 118, # 11 p. 4459 - 4472
反应条件
silver fluoride; chlorine
参考文献
Chambers,W.J. et al.
Journal of the American Chemical Society, 1962 , vol. 84, p. 2337 - 2343
反应条件
potassium fluoride in further solvent(s)
with fluorination in tetramethylene sulfone at 60°C for 70 h;
参考文献
Cameron, J. D.; Tattershall, B. W.
Angewandte Chemie, 1975 , vol. 87, p. 208 - 209
反应条件
chlorine
at 75-140°C under pressure;
参考文献
Chambers,W.J. et al.
Journal of the American Chemical Society, 1962 , vol. 84, p. 2337 - 2343
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Gmelin Handbook: C: MVol.D3, 6.2.4.7.7.8, page 214 - 215