9-磷杂二环[3.3.1]壬烷合成路线 （共 3 条）
反应条件
VAZO-52 in toluene T=60 - 600°C;
参考文献
Yaowu, Sha
Patent: US2004/138504 A1, 2004 ;
Location in patent: Page 6 ;
反应条件
1: With sodium hydroxide in water pH=8.5; 0.5 h; 2: With sodium hydroxide; sodium hydrogensulfite in water; toluene pH=12; 0.5 h;
参考文献
Yaowu, Sha
Patent: US2004/138504 A1, 2004 ;
Location in patent: Page 6 ;
反应条件
1,2,2-trichloro-1,1,2-trichloro-ethane in toluene T=90 - 115°C;
参考文献
Carreira, Monica; Charernsuk, Manutsavin; Eberhard, Michael; Fey, Natalie; Ginkel, Roel van; et al.
Journal of the American Chemical Society, 2009 , vol. 131, p. 3078 - 3092
