3,6,9-三噁十一烷二酸合成路线 （共 7 条）
反应条件
trifluoroacetic acid in dichloromethane 2 h; Ambient temperature;
参考文献
Bright, Sandra A.; Brinko, Anne; Larsen, Maja Thim; Sinning, Steffen; Williams, D. Clive; Jensen, Henrik H.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 5 p. 1220 - 1224
反应条件
T=5°C; 8 h; electrolysis: nickel net anode, cylindrical stainless steel cathode; electrolyte: 1M NaOH/H2O; Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 38, # 22 p. 3299 - 3308
参考文献
Tetrahedron, , vol. 38, # 14 p. 2055 - 2060
反应条件
pyridine; oxalyl dichloride in benzene 24 h; Ambient temperature;
参考文献
Sato, Masayuki; Oda, Tsunehisa; Iwamoto, Ken-ichi; Fujii, Satoshi
Heterocycles, 2003 , vol. 60, # 4 p. 899 - 908
反应条件
pyridine O-ethylphosphoric dichloride
T=20 - 50°C; 24 h; Yield given;
参考文献
Biernat, Jan F.; Luboch, Elzbieta
Tetrahedron, 1984 , vol. 40, # 10 p. 1927 - 1930
反应条件
1: pyridine O-ethylphosphoric dichloride / 24 h / 20 - 50 °C
2: 60 percent / benzene / 6.5 h / Heating
3: 60 percent / LiAlH4 / tetrahydrofuran / 96 h
View Scheme
参考文献
Biernat, Jan F.; Luboch, Elzbieta
Tetrahedron, 1984 , vol. 40, # 10 p. 1927 - 1930
反应条件
1: pyridine O-ethylphosphoric dichloride / 24 h / 20 - 50 °C
2: 50 percent / benzene / 6.5 h / Heating
3: 90 percent / LiAlH4 / tetrahydrofuran / 96 h
View Scheme
参考文献
Biernat, Jan F.; Luboch, Elzbieta
Tetrahedron, 1984 , vol. 40, # 10 p. 1927 - 1930
