反应条件
in tetrahydrofuran under N2, 24 h stirring at reflux, cooled to 25°C,quenched with MeOH, pptn. by addn. of heptane; filtered, freed of volatike solvent, dark residue redigested with warm heptane, filtered, solvent removal, recrystn. from acetonitrile and charcoal, repeated recrystn. from CH3CN-CH2Cl2, elem. anal.;
参考文献
Eisch, John J.; Shafii, Babak; Odom, Jerome D.; Rheingold, Arnold L.
Journal of the American Chemical Society, 1990 , vol. 112, # 5 p. 1847 - 1853
