甲基(3Z)-3-己烯酸酯合成路线 (共 14 条)
反应条件
hydrogen; tricarbonyl(.eta.(6)-1,2,3-trimethoxybenzene)chromium in tetrahydrofuran T=80°C; P=45600 Torr; 5 h; different catalysts, different temperatures;
参考文献
Maux, P. Le; Saillard, J.Y.; Grandjean, D.; Jaouen, G.
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4524 - 4526
反应条件
polyethylene glycol; sodium tetrahydroborate; palladium dichloride in dichloromethane T=10°C; P=735.5 Torr; 1 h; further solvent: EtOH; further catalyst: Pd/C; Product distribution;
参考文献
Suzuki, Nobutaka; Tsukanaka, Tsuneaki; Nomoto, Tateo; Ayaguchi, Yasuo; Izawa, Yasuji
Journal of the Chemical Society, Chemical Communications, 1983 , # 9 p. 515 - 516
反应条件
sodium tetrahydroborate; palladium dichloride in dichloromethane T=10°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Suzuki, N.; Kaneko, Y.; Tsukanaka, T.; Nomoto, T.; Ayaguchi, Y.; Izawa, Y.
Tetrahedron, 1985 , vol. 41, # 12 p. 2387 - 2392
反应条件
sodium tetrahydroborate; palladium on activated charcoal in ethanol T=10°C; 2.25 h; Yield given. Yields of byproduct given;
参考文献
Suzuki, N.; Kaneko, Y.; Tsukanaka, T.; Nomoto, T.; Ayaguchi, Y.; Izawa, Y.
Tetrahedron, 1985 , vol. 41, # 12 p. 2387 - 2392
反应条件
1: H2, quinoline / Lindlar / ethyl acetate View Scheme
参考文献
Ansell,M.F. et al.
Journal of the Chemical Society [Section] C: Organic, 1968 , p. 217 - 225
反应条件
1: 4.85 g / 8 M CrO3 / acetone / Ambient temperature 2: 98percent H2SO4 / 18 h / Heating View Scheme
参考文献
Landais, Yannick; Planchenault, Denis; Weber, Valery
Tetrahedron Letters, 1994 , vol. 35, # 51 p. 9549 - 9552
反应条件
hydrogen; Cr catalyst
参考文献
Eden,Y. et al.
Israel Journal of Chemistry, 1976 , vol. 15, p. 223 - 229
反应条件
sulfuric acid 18 h; Heating;
参考文献
Azzena, Francesca; Crotti, Paolo; Favero, Lucilla; Pineschi, Mauro
Tetrahedron, 1995 , vol. 51, # 48 p. 13409 - 13422
反应条件
hydrogenchloride; bis(1,5-cyclooctadiene)nickel (0); dcype 1.) THF, RT, 48 h, 2.) 20 deg C, 16 h; Multistep reaction;
参考文献
Hoberg, H.; Schaefer, D.; Oster, B. W.
Journal of Organometallic Chemistry, 1984 , vol. 266, # 3 p. 313 - 320
参考文献
Ansell,M.F. et al.
Journal of the Chemical Society [Section] C: Organic, 1968 , p. 217 - 225
Full Text View citing articles Show Details
Landais, Yannick; Planchenault, Denis; Weber, Valery
Tetrahedron Letters, 1994 , vol. 35, # 51 p. 9549 - 9552