N-(3-氯苯基)甲酰胺合成路线 (共 21 条)
反应条件
nickel in ethanol 1 h; Heating;
参考文献
Ali, M. Umar; Meshram, H. M.; Paranjpe, M. G.
Journal of the Indian Chemical Society, 1985 , vol. 62, # 9 p. 666 - 669
反应条件
sodium hydroxide; water in 1,4-dioxane T=70°C; isotope effect (D2O); ΔH(excit.), ΔS(excit.); MechanismKineticsThermodynamic data;
参考文献
Cunningham, Ian D.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1485 - 1490
反应条件
1: KOH; ethanol / anschliessendes Behandeln mit wss. HCl 2: Erhitzen des Reaktionsprodukts mit wss. HCl 4: NaNH2; diethyl ether View Scheme
参考文献
Koenig; Huisgen
Chemische Berichte, 1959 , vol. 92, p. 429,435
反应条件
lithium aluminium tetrahydride in tetrahydrofuran Ambient temperature;
参考文献
Rosowsky, Andre; Forsch, Ronald A.; Queener, Sherry F.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 14 p. 2615 - 2620
反应条件
potassium hydroxide; ethanol anschliessendes Behandeln mit wss. HCl;
参考文献
Koenig; Huisgen
Chemische Berichte, 1959 , vol. 92, p. 429,435
反应条件
bis(trichloromethyl) carbonate; triethylamine in dichloromethane T=-10°C; 0.5 h;
参考文献
Yu, Shu-Jing; Zhu, Cong; Bian, Qiang; Cui, Can; Du, Xiu-Jiang; Li, Zheng-Ming; Zhao, Wei-Guang
ACS Combinatorial Science, 2014 , vol. 16, # 1 p. 17 - 23
反应条件
sodium hydroxide; water in 1,4-dioxane T=70°C; isotope effect (D2O); ΔH(excit.), ΔS(excit.); KineticsThermodynamic data;
参考文献
Cunningham, Ian D.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1485 - 1490
参考文献
Price; Roberts
Journal of the American Chemical Society, 1946 , vol. 68, p. 1255
反应条件
ethanol; sodium ethanolate; phosphorus trichoride Multistep reaction;
参考文献
Ali, M. Umar; Paranjpe, M. G.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 6 p. 573 - 574
参考文献
Jentzsch,W.
Chemische Berichte, 1964 , vol. 97, p. 1361 - 1368