(S)-N-Boc-2,2-二甲基噁唑烷-4-甲酸合成路线 （共 12 条）
反应条件
benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide
参考文献
Temperini, Andrea; Capperucci, Antonella; Degl'Innocenti, Alessandro; Terlizzi, Raffaella; Tiecco, Marcello
Tetrahedron Letters, 2010 , vol. 51, # 31 p. 4121 - 4124
反应条件
1: Garner's aldehyde With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane T=20°C; Inert atmosphere; 2: pentadec-1-yne With n-butyllithium in tetrahydrofuran T=-78°C; 0.25 h; Inert atmosphere; 3: in tetrahydrofuran T=-78 - 20°C; 0.25 h; Inert atmosphereEnzymatic reaction;
参考文献
Morales-Serna, Jose Antonio; Sauza, Alejandro; Padron De Jesus, Gabriela; Gavino, Ruben; Garcia De La Mora, Gustavo; Cardenas, Jorge
Tetrahedron Letters, 2013 , vol. 54, # 52 p. 7111 - 7114
