1,2,3,4,5-戊甲氧基苯合成路线 （共 5 条）
反应条件
1: AlCl3, aluminium chloride / dichloromethane / 0 - 20 °C 2: lithium hexamethyldisilazane / tetrahydrofuran / -30 - 0 °C / Inert atmosphere 3: trifluoroacetic acid / methanol / 24 h / 50 °C View Scheme
参考文献
Chemical Communications, , vol. 47, # 10 p. 2868 - 2870
反应条件
pyridine-2-carboxylic acid, Ag(II) salt in water; benzene 3 h; Ambient temperature;
参考文献
Syper, Ludwik; Kloc, Krystian; Mlochowski, Jacek
Journal fuer Praktische Chemie (Leipzig), 1985 , vol. 327, # 5 p. 808 - 822
反应条件
1: AlCl3, aluminium chloride / dichloromethane / 0 - 20 °C 2: lithium hexamethyldisilazane / tetrahydrofuran / -30 - 0 °C / Inert atmosphere 3: trifluoroacetic acid / methanol / 24 h / 50 °C 4: AlCl3, aluminium chloride; ethanethiol / CHCl2 / 0 - 20 °C View Scheme
参考文献
Chemical Communications, , vol. 47, # 10 p. 2868 - 2870
反应条件
In(OSO2CF3)3
T=145 - 160°C; Friedel-Crafts acetylation; 0.25 h; IrradiationMicrowave;
参考文献
Tsukayama, Masao; Kusunoki, Eiji; Hossain, Mohammad M.; Kawamura, Yasuhiko; Hayashi, Shinji
Heterocycles, 2007 , vol. 71, # 7 p. 1589 - 1600
反应条件
In(OSO2CF3)3
0.25 h; microwave irradiation;
参考文献
Tsukayama, Masao; Kawamura, Yasuhiko; Ishizuka, Takaaki; Hayashi, Shinji; Torii, Fumihito
Heterocycles, 2003 , vol. 60, # 12 p. 2775 - 2784
