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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
13910-11-7
合成路线
（共 17 条）
13910-11-7
→
反应条件
1918-88-3
反应条件
cyclohexane-1,1-diyl bis-hydro peroxide in dichloromethane T=20°C; 2 h;
参考文献
Jon Paul Selvam; Suresh; Rajesh; Chanti Babu; Suryakiran; Venkateswarlu
Tetrahedron Letters, 2008 , vol. 49, # 21 p. 3463 - 3465
10276-04-7
[(3-甲基丁-2-烯-1-基)硫代]苯
→
反应条件
13910-11-7
+
108-98-5
硫酚
反应条件
hydrogen; lt;Ru3O(CH3COO)6(H2O)3gt;(1+)*CH3COO(1-) in N,N-dimethyl-formamide T=80°C; P=3040 Torr; 2 h; other catalyst: RuO2*nH2O;
参考文献
Cere, Vanda; Massaccesi, Franco; Pollicino, Salvatore; Ricci, Alfredo
Synthetic Communications, 1996 , vol. 26, # 5 p. 899 - 907
4285-49-8
→
反应条件
13910-11-7
反应条件
1: 5 percent / hydrogen / RuO2*nH2O / methanol / 48 h / 60 °C / 6080 Torr 2: hydrogen / <Ru3O(CH3COO)6(H2O)3>(1+)*CH3COO(1-) / dimethylformamide / 2 h / 80 °C / 3040 Torr 3: Na, ethanol / Ambient temperature 4: 4 percent / hydrogen / <Ru3O(CH3COO)6(H2O)3>(1+)*CH3COO(1-) / dimethylformamide / 2 h / 80 °C / 3040 Torr / other catalyst: RuO2*nH2O View Scheme
参考文献
Cere, Vanda; Massaccesi, Franco; Pollicino, Salvatore; Ricci, Alfredo
Synthetic Communications, 1996 , vol. 26, # 5 p. 899 - 907
5296-64-0
烯丙氧基苯硫酚
→
反应条件
13910-11-7
反应条件
1: hydrogen / <Ru3O(CH3COO)6(H2O)3>(1+)*CH3COO(1-) / dimethylformamide / 2 h / 80 °C / 3040 Torr / other catalyst: RuO2*nH2O 2: Na, ethanol / Ambient temperature 3: 4 percent / hydrogen / <Ru3O(CH3COO)6(H2O)3>(1+)*CH3COO(1-) / dimethylformamide / 2 h / 80 °C / 3040 Torr / other catalyst: RuO2*nH2O View Scheme
参考文献
Cere, Vanda; Massaccesi, Franco; Pollicino, Salvatore; Ricci, Alfredo
Synthetic Communications, 1996 , vol. 26, # 5 p. 899 - 907
702-04-5
→
反应条件
13910-11-7
反应条件
1: hydrogen / <Ru3O(CH3COO)6(H2O)3>(1+)*CH3COO(1-) / dimethylformamide / 2 h / 80 °C / 3040 Torr 2: Na, ethanol / Ambient temperature 3: 4 percent / hydrogen / <Ru3O(CH3COO)6(H2O)3>(1+)*CH3COO(1-) / dimethylformamide / 2 h / 80 °C / 3040 Torr / other catalyst: RuO2*nH2O View Scheme
参考文献
Cere, Vanda; Massaccesi, Franco; Pollicino, Salvatore; Ricci, Alfredo
Synthetic Communications, 1996 , vol. 26, # 5 p. 899 - 907
1822-73-7
苯基乙烯基硫醚
→
反应条件
13910-11-7
反应条件
1: hydrogen / RuO2*nH2O / methanol / 48 h / 60 °C / 6080 Torr / other catalyst: <Ru3O(CH3COO)6(H2O)3>(1+)*CH3COO(1-) 2: Na, ethanol / Ambient temperature 3: 4 percent / hydrogen / <Ru3O(CH3COO)6(H2O)3>(1+)*CH3COO(1-) / dimethylformamide / 2 h / 80 °C / 3040 Torr / other catalyst: RuO2*nH2O View Scheme
参考文献
Cere, Vanda; Massaccesi, Franco; Pollicino, Salvatore; Ricci, Alfredo
Synthetic Communications, 1996 , vol. 26, # 5 p. 899 - 907
10276-04-7
[(3-甲基丁-2-烯-1-基)硫代]苯
→
反应条件
13910-11-7
反应条件
1: hydrogen / <Ru3O(CH3COO)6(H2O)3>(1+)*CH3COO(1-) / dimethylformamide / 2 h / 80 °C / 3040 Torr / other catalyst: RuO2*nH2O 2: Na, ethanol / Ambient temperature View Scheme
参考文献
Cere, Vanda; Massaccesi, Franco; Pollicino, Salvatore; Ricci, Alfredo
Synthetic Communications, 1996 , vol. 26, # 5 p. 899 - 907
108-98-5
硫酚
→
反应条件
13910-11-7
反应条件
1: Na, ethanol / Ambient temperature 2: 4 percent / hydrogen / <Ru3O(CH3COO)6(H2O)3>(1+)*CH3COO(1-) / dimethylformamide / 2 h / 80 °C / 3040 Torr / other catalyst: RuO2*nH2O View Scheme
参考文献
Cere, Vanda; Massaccesi, Franco; Pollicino, Salvatore; Ricci, Alfredo
Synthetic Communications, 1996 , vol. 26, # 5 p. 899 - 907
3111-52-2
苯硫酚钾
+
107-82-4
1-溴代异戊烷
→
反应条件
13910-11-7
反应条件
ethanol
参考文献
Ipatieff; Pines; Friedman
Journal of the American Chemical Society, 1938 , vol. 60, p. 2732
543-50-0
→
反应条件
1013-88-3
二苯甲酮亚胺
+
13910-11-7
反应条件
diethyl ether
参考文献
Adams; Bramlet; Tendick
Journal of the American Chemical Society, 1920 , vol. 42, p. 2374
Journal of the American Chemical Society, 1922 , vol. 44, p. 873
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