pyridinium chlorochromate in dichloromethane T=25°C; 2 h; Inert atmosphere;
参考文献
Ueno, Yuichiro; Jose, Jiney; Loudet, Aurore; Perez-Bolivar, Cesar; Anzenbacher, Pavel; Burgess, Kevin
Journal of the American Chemical Society, 2011 , vol. 133, # 1 p. 51 - 55
1: AlH3 / tetrahydrofuran / 1.) reflux, 25.5 h, 2.) RT, 91 h 2: pyridinium dichromate / CH2Cl2 / 51 h / Ambient temperature View Scheme
参考文献
Ueno, Yuichiro; Jose, Jiney; Loudet, Aurore; Perez-Bolivar, Cesar; Anzenbacher, Pavel; Burgess, Kevin
Journal of the American Chemical Society, 2011 , vol. 133, # 1 p. 51 - 55
1: potassium carbonate / acetone / 20 h / 60 °C / Inert atmosphere 2: diisobutylaluminium hydride / tetrahydrofuran / -78 - 25 °C / Inert atmosphere 3: pyridinium chlorochromate / dichloromethane / 2 h / 25 °C / Inert atmosphere View Scheme
参考文献
Ueno, Yuichiro; Jose, Jiney; Loudet, Aurore; Perez-Bolivar, Cesar; Anzenbacher, Pavel; Burgess, Kevin
Journal of the American Chemical Society, 2011 , vol. 133, # 1 p. 51 - 55