1,4-二氯丁烷-2S-3S-二醇合成路线 (共 9 条)
反应条件
methanesulfonamide; sodium hydrogencarbonate; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III) in water; tert-butyl alcohol T=0°C; Yield given. Yields of byproduct given;
参考文献
Choudary; Chowdari; Kantam; Raghavan
Journal of the American Chemical Society, 2001 , vol. 123, # 37 p. 9220 - 9221
反应条件
methanesulfonyl chloride; triethylamine; lithium chloride in acetonitrile Heating;
参考文献
Kim; Bae; So; Yoo; Chang; Lee; Kang
Organic letters, 2001 , vol. 3, # 15 p. 2349 - 2351
反应条件
AD-mix-β; sodium hydrogencarbonate in water; tert-butyl alcohol T=0°C; asymmetric dihydroxylation under Sharpless' buffered conditions;
参考文献
Kim, B. Moon; Bae, Sung Jin; Seomoon, Gunn
Tetrahedron Letters, 1998 , vol. 39, # 38 p. 6921 - 6922
反应条件
hydrogenchloride in diethyl ether
参考文献
Feit,P.W.
Chemische Berichte, 1960 , vol. 93, p. 116 - 127
反应条件
sodium hydroxide in methanol; diethyl ether; water 1 h;
参考文献
Vanhessche, Koen P. M.; Wang, Zhi-Min; Sharpless, K. Barry
Tetrahedron Letters, 1994 , vol. 35, # 21 p. 3469 - 3472
反应条件
sodium hydroxide in methanol; diethyl ether; water 1 h;
参考文献
Vanhessche, Koen P. M.; Wang, Zhi-Min; Sharpless, K. Barry
Tetrahedron Letters, 1994 , vol. 35, # 21 p. 3469 - 3472
反应条件
sodium hydroxide in methanol; diethyl ether; water 1 h;
参考文献
Vanhessche, Koen P. M.; Wang, Zhi-Min; Sharpless, K. Barry
Tetrahedron Letters, 1994 , vol. 35, # 21 p. 3469 - 3472
反应条件
sodium hydroxide in methanol; diethyl ether; water 1 h;
参考文献
Vanhessche, Koen P. M.; Wang, Zhi-Min; Sharpless, K. Barry
Tetrahedron Letters, 1994 , vol. 35, # 21 p. 3469 - 3472
反应条件
1: With thionyl chloride in tetrachloromethane 0.5 h; Heating; 2: With ruthenium trichloride; sodium periodate in tetrachloromethane; water; acetonitrile T=0°C; 1 h; Further stages.;
参考文献
Kim; Bae; So; Yoo; Chang; Lee; Kang
Organic letters, 2001 , vol. 3, # 15 p. 2349 - 2351