(3-溴-5-硝基苯基)甲醇合成路线 （共 5 条）
反应条件
1: With borane-THF in tetrahydrofuran T=0 - 20°C; 2: With methanol in tetrahydrofuran T=0°C;
参考文献
Reuter, Raphael; Wegner, Hermann A.
Chemical Communications, 2013 , vol. 49, # 2 p. 146 - 148
反应条件
1: N-bromosuccinmide; sulfuric acid / 20 h / 60 °C 2: dimethylsulfide borane complex / tetrahydrofuran / -15 - 60 °C / Inert atmosphere View Scheme
参考文献
Reuter, Raphael; Wegner, Hermann A.
Chemical Communications, 2013 , vol. 49, # 2 p. 146 - 148
反应条件
oxygen; caesium carbonate in water 2 h; Reflux;
参考文献
Albadi, Jalal; Alihoseinzadeh, Amir; Razeghi, Abdolhosein
Catalysis Communications, 2014 , vol. 49, p. 1 - 5
反应条件
N-bromosuccinmide; triphenylphosphine in tetrahydrofuran T=0 - 20°C; 16 h;
参考文献
Bristol-Myers Squibb Company
Patent: US2007/249607 A1, 2007 ;
Location in patent: Page/Page column 90 ;
US 20070249607 A1
反应条件
phosphorus pentachloride in chloroform 12 h; Heating;
参考文献
Lahiri; Thompson; Moore
Journal of the American Chemical Society, 2000 , vol. 122, # 46 p. 11315 - 11319
