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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1-萘硼酸
合成路线
（共 242 条）
109-04-6
邻溴吡啶
+
13922-41-3
1-萘硼酸
→
反应条件
76759-26-7
2-萘基吡啶
反应条件
potassium tert-butylate; ClPd[N,N(2,6-iPr2C6H3)2-imidazol-2-yl]cinnamyl in isopropyl alcohol T=20°C; Suzuki-Miyaura cross-coupling reaction; 3.5 h;
参考文献
Navarro, Oscar; Marion, Nicolas; Mei, Jianguo; Nolan, Steven P.
Chemistry - A European Journal, 2006 , vol. 12, # 19 p. 5142 - 5148
109-09-1
2-氯吡啶
+
13922-41-3
1-萘硼酸
→
反应条件
76759-26-7
2-萘基吡啶
反应条件
potassium phosphate; palladium diacetate in tetrahydrofuran T=100°C; Suzuki-Miyaura coupling; 24 h;
参考文献
Chau, Ming So; Chung, Chiu Yeung; Chak, Po Lau; Fuk, Yee Kwong
Journal of Organic Chemistry, 2008 , vol. 73, # 19 p. 7803 - 7806
109-04-6
邻溴吡啶
+
201230-82-2
+
13922-41-3
1-萘硼酸
→
反应条件
76759-26-7
2-萘基吡啶
+
107341-55-9
反应条件
caesium carbonate; 1,3-bis(2,4,6-trimethylphenyl)imidazolinium chloride; palladium diacetate in 1,4-dioxane T=120°C; P=37503 Torr; 15 h;
参考文献
Maerten, Eddy; Sauthier, Mathieu; Mortreux, Andre; Castanet, Yves
Tetrahedron, 2007 , vol. 63, # 3 p. 682 - 689
25795-97-5
+
13922-41-3
1-萘硼酸
→
反应条件
76759-26-7
2-萘基吡啶
反应条件
1-methyl-2-(2-(dicyclohexylphosphino)phenyl)-1H-benzoimidazole; palladium diacetate; sodium carbonate in tert-butyl alcohol T=20 - 120°C; Suzuki-Miyaura coupling; 18 h;
参考文献
Chung, Kin Ho; So, Chau Ming; Wong, Shun Man; Luk, Chi Him; Zhou, Zhongyuan; Lau, Chak Po; Kwong, Fuk Yee
Chemical Communications, 2012 , vol. 48, # 14 p. 1967 - 1969
142-08-5
2-羟基吡啶
+
13922-41-3
1-萘硼酸
→
反应条件
76759-26-7
2-萘基吡啶
反应条件
1: 2-hydroxy-pyridine With potassium carbonate; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate in 1,4-dioxane T=100°C; 3 h; Inert atmosphere; 2: naphthalene-1-boronic acid With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane; water T=100°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Li, Shui-Ming; Huang, Jie; Chen, Guo-Jun; Han, Fu-She
Chemical Communications, 2011 , vol. 47, # 48 p. 12840 - 12842
13922-41-3
1-萘硼酸
→
反应条件
76759-26-7
2-萘基吡啶
反应条件
1.1: dichloromethane / 0.5 h / 20 °C / |Inert atmosphere 1.2: 0.25 h / 20 °C / |Inert atmosphere 2.1: triethylamine / tetrahydrofuran / 18 h / 0 - 20 °C / |Inert atmosphere 3.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / ethanol / 18 h / 100 °C / |Inert atmosphere View Scheme
参考文献
Goggins, Sean; Rosevere, Eleanor; Bellini, Clement; Allen, Joseph C.; Marsh, Barrie J.; Mahon, Mary F.; Frost, Christopher G.
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 1 p. 47 - 52
13922-41-3
1-萘硼酸
+
298-12-4
乙醛酸
+
76-05-1
三氟乙酸
→
反应条件
772-84-9
反应条件
Multistep reaction.;
参考文献
Gravel, Michael; Thompson, Kim A.; Zak, Mark; Berube, Christian; Hall, Dennis G.
Journal of Organic Chemistry, 2002 , vol. 67, # 1 p. 3 - 15
504-61-0
巴豆醇
+
13922-41-3
1-萘硼酸
→
反应条件
78237-60-2
反应条件
tetrakis(triphenylphosphine) palladium(0) in dichloromethane T=80°C; 9 h; Title compound not separated from byproducts;
参考文献
Tsukamoto, Hirokazu; Uchiyama, Tomomi; Suzuki, Takamichi; Kondo, Yoshinori
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 16 p. 3005 - 3013
598-32-3
+
13922-41-3
1-萘硼酸
→
反应条件
78237-60-2
反应条件
tetrakis(triphenylphosphine) palladium(0) in dichloromethane T=80°C; 9 h; Title compound not separated from byproducts;
参考文献
Tsukamoto, Hirokazu; Uchiyama, Tomomi; Suzuki, Takamichi; Kondo, Yoshinori
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 16 p. 3005 - 3013
598-32-3
+
13922-41-3
1-萘硼酸
→
反应条件
78237-60-2
反应条件
tetrakis(triphenylphosphine) palladium(0) in dichloromethane T=80°C; 9 h; Title compound not separated from byproducts;
参考文献
Tsukamoto, Hirokazu; Sato, Masanori; Kondo, Yoshinori
Chemical Communications, 2004 , # 10 p. 1200 - 1201
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