1: 96 percent / NaBr / dimethylformamide / 1 h / 50 °C
3: 98 percent / LiAlH4 / diethyl ether / 0.17 h / 0 °C
4: 100 percent / MeSiBr / ZnBr / CH2Cl2 / 0.33 h / 0 °C
5: 89 percent / dibenzo-18-crown-6 / acetonitrile / 15 h / Heating
View Scheme
参考文献
Moiseenkov, Alexander M.; Czeskis, Boris A.; Ivanova, Natalya M.; Nefedov, Oleg M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , p. 2639 - 2649