Fmoc-11-氨基-3,6,9-三噁十一酸合成路线 （共 9 条）
反应条件
potassium carbonate in water T=20°C; 16.75 h;
参考文献
Schmidt, Florian; Rosnizeck, Ina C.; Spoerner, Michael; Kalbitzer, Hans Robert; Koenig, Burkhard
Inorganica Chimica Acta, 2011 , vol. 365, # 1 p. 38 - 48
反应条件
1: 2-lt;2-lt;2-(aminoethoxy)ethoxygt;ethoxygt;acetic acid With potassium carbonate in water T=20°C; 0.25 h; 2: 1-[[(9H-fluoren-9-ylmethoxy)carbonyl]oxy]-2,5-pyrrolidinedione in water 24 h;
参考文献
Gomez, Francisco L. Guerra; Uehara, Tomoya; Rokugawa, Takemi; Higaki, Yusuke; Suzuki, Hiroyuki; Hanaoka, Hirofumi; Akizawa, Hiromichi; Arano, Yasushi
Bioconjugate Chemistry, 2012 , vol. 23, # 11 p. 2229 - 2238
反应条件
sodium hydrogencarbonate in 1,4-dioxane; water 1.) 0 deg C, 2 h, 2.) room temperature, 48 h;
参考文献
Boumrah, Derradji; Campbell, Malcolm M.; Fenner, Simon; Kinsman, Richard G.
Tetrahedron, 1997 , vol. 53, # 20 p. 6977 - 6992
反应条件
1: dichloromethane 2: sodium hydroxide / tetrahydrofuran; toluene / 45 °C 3: hydrogenchloride; water / 1 h 4: potassium carbonate / water / 16.75 h / 20 °C View Scheme
参考文献
Inorganica Chimica Acta, , vol. 365, # 1 p. 38 - 48
反应条件
1: palladium on carbon; hydrogen / tetrahydrofuran 2: dichloromethane 3: sodium hydroxide / tetrahydrofuran; toluene / 45 °C 4: hydrogenchloride; water / 1 h 5: potassium carbonate / water / 16.75 h / 20 °C View Scheme
参考文献
Inorganica Chimica Acta, , vol. 365, # 1 p. 38 - 48
反应条件
1: sodium azide / N,N-dimethyl-formamide / 20 °C 2: palladium on carbon; hydrogen / tetrahydrofuran 3: dichloromethane 4: sodium hydroxide / tetrahydrofuran; toluene / 45 °C 5: hydrogenchloride; water / 1 h 6: potassium carbonate / water / 16.75 h / 20 °C View Scheme
参考文献
Inorganica Chimica Acta, , vol. 365, # 1 p. 38 - 48
反应条件
1: sodium hydroxide / tetrahydrofuran; toluene / 45 °C 2: hydrogenchloride; water / 1 h 3: potassium carbonate / water / 16.75 h / 20 °C View Scheme
参考文献
Inorganica Chimica Acta, , vol. 365, # 1 p. 38 - 48
反应条件
1: hydrogenchloride; water / 1 h 2: potassium carbonate / water / 16.75 h / 20 °C View Scheme
参考文献
Inorganica Chimica Acta, , vol. 365, # 1 p. 38 - 48
反应条件
1: sodium hydroxide 2: sodium azide / N,N-dimethyl-formamide / 20 °C 3: palladium on carbon; hydrogen / tetrahydrofuran 4: dichloromethane 5: sodium hydroxide / tetrahydrofuran; toluene / 45 °C 6: hydrogenchloride; water / 1 h 7: potassium carbonate / water / 16.75 h / 20 °C View Scheme
参考文献
Inorganica Chimica Acta, , vol. 365, # 1 p. 38 - 48
