反应条件
1.1: hydrazine hydrate / ethanol / 4 h / Reflux
2.1: hydrogen / palladium 10 on activated carbon / ethanol; water / 12 h / 20 °C / 760.05 Torr
3.1: triethylamine / dichloromethane / 3 h / 0 - 20 °C
4.1: hydrogenchloride; water; acetic acid / 1 h / 25 °C
4.2: pH 9 / Cooling with ice
View Scheme