trimethylsilylazide in dichloromethane; 1,2-dichloro-ethane T=25°C; 1 h;
参考文献
Gray, Michael A.; Rees, Charles W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 24 p. 3077 - 3080
in dichloromethane T=22°C; 8 h; effect of increased reagent concentration and reduced addition time on yield and volume efficiency; Product distribution;
参考文献
Rees, Charles W.; Surtees, John R. J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 2945 - 2953
Rees, Charles W.; Surtees, John R. J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 12 p. 2945 - 2953