4-氯-5-(2,3-二氯苯氧基)-1,2-苯二胺合成路线 （共 7 条）
反应条件
hydrogen in ethanol T=25°C;
参考文献
SEQUENT SCIENTIFIC LIMITED; Rane, Ramkrishna Appaji; Verma, Sudhakar; Arulmoli, Thangavel
Patent: US2013/303781 A1, 2013 ;
Location in patent: Paragraph 0025 ;
反应条件
sodium dithionite in ethanol Heating;
参考文献
Iddon, Brian
Bulletin des Societes Chimiques Belges, 1990 , vol. 99, # 9 p. 673 - 701
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 90 °C / Industry scale 2: sodium hydroxide; water / methanol / 4 h / 50 °C / Industry scale 3: hydrogen; sodium hydroxide / Raney nickel / methanol / 12 h / 100 °C / Industry scale View Scheme
参考文献
SEQUENT SCIENTIFIC LIMITED; Rane, Ramkrishna Appaji; Verma, Sudhakar; Arulmoli, Thangavel
Patent: US2013/303781 A1, 2013 ;
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 90 °C / Industry scale 2: sodium hydroxide; water / methanol / 4 h / 50 °C / Industry scale 3: hydrogen; sodium hydroxide / Raney nickel / methanol / 12 h / 100 °C / Industry scale View Scheme
参考文献
SEQUENT SCIENTIFIC LIMITED; RANE, Ramkrishna Appaji; VERMA, Sudhakar; ARULMOLI, Thangavel
Patent: WO2012/70068 A2, 2012 ;
反应条件
1: 60 percent / methanol 2: 89 percent / Na2S2O4 / aq. ethanol / Heating View Scheme
参考文献
Iddon, Brian
Bulletin des Societes Chimiques Belges, 1990 , vol. 99, # 9 p. 673 - 701
反应条件
1: 60 percent / methanol 2: 89 percent / Na2S2O4 / aq. ethanol / Heating View Scheme
参考文献
Iddon, Brian
Bulletin des Societes Chimiques Belges, 1990 , vol. 99, # 9 p. 673 - 701
反应条件
1.1: methanol / 6 h / |Reflux 1.2: 4 h / 60 - 90 °C 2.1: methanol; water / 0.5 h / 60 °C 2.2: 1.5 h / 60 °C View Scheme
参考文献
SEQUENT SCIENTIFIC LIMITED; Rane, Ramkrishna Appaji; Verma, Sudhakar; Arulmoli, Thangavel
Patent: US2013/303781 A1, 2013 ;
