反应条件
in acetonitrile byproducts: CO; under Ar: mixt. of Mo(CO)6 and Na(O2CMe) in MeCN stirred rapidly, addn. of NOBF4 in MeCN, allowed to react (2 h, room temp.); filtered, concd. (vac., 1/2 vol.), treated with CH2Cl2, white ppt. filtered off, filtrate treated with CH2Cl2, filtered, addn. of hexane, filtered, washed (hexane and CH2Cl2), dried (vac.), elem. anal.;
参考文献
Journal of molecular catalysis, , vol. 53, # 3 p. L9-L11
