(二苯基甲基硅烷基)乙酸乙酯合成路线 (共 6 条)
反应条件
zinc in diethyl ether
参考文献
Albaugh-Robertson, Pamela; Katzenellenbogen, John A.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5288 - 5302
反应条件
C2H3CuN(1+)*C9HBBr9N6(1-) in dichloromethane T=20°C; 12 h;
参考文献
Iglesias, M. Jose; Nicasio, M. Carmen; Caballero, Ana; Perez, Pedro J.
Dalton Transactions, 2013 , vol. 42, # 4 p. 1191 - 1195
反应条件
lithium diisopropyl amide in tetrahydrofuran; hexane 1.) -78 deg C, 40 min, 2.) -78 deg C, 1 h, room temperature;
参考文献
Larson, Gerald L.; Quiroz, Fernando; Suarez, Juan
Synthetic Communications, 1983 , vol. 13, # 10 p. 833 - 844
反应条件
T=360.1°C; other temperature; Rate constant;
参考文献
Chapman, Sara E.; Taylor, Roger
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , p. 1119 - 1120
反应条件
lithium diisopropyl amide 1.) THF, -78 deg C; Yield given. Multistep reaction;
参考文献
Larson,G.L.; Fuentes,L.M.
Journal of the American Chemical Society, 1981 , vol. 103, p. 2418
反应条件
T=360.1°C; other temperature; Rate constant;
参考文献
Chapman, Sara E.; Taylor, Roger
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , p. 1119 - 1120