2-(7-甲氧基萘-1-基)乙胺盐酸盐合成路线 （共 35 条）
反应条件
1: hydrogen; ammonia / Raney nickel / ethanol; water / 3 h / 40 °C / Autoclave vessel 2: hydrogenchloride / ethyl acetate / 0.5 h / 0 - 5 °C 3: sulfur / 0.5 h / 180 - 185 °C View Scheme
反应条件
1: pyridine / 3 h / -5 - 0 °C 2: N,N-dimethyl-formamide / 2 h / Reflux 3: hydrazine hydrate / ethanol / 2 h / Reflux View Scheme
反应条件
1.1: potassium carbonate / acetone / 2.25 h / 28 - 55 °C 2.1: AlCl3, aluminium chloride / dichloromethane / 0.67 h / 0 °C 2.2: 5.5 h / -10 °C 3.1: triethylsilane / dichloromethane / 20 - 25 °C 3.2: 3 h / -10 - 0 °C 3.3: 2.16 h / 25 °C 4.1: potassium carbonate / methanol / 28 °C 4.2: 2.4 h / 15 - 25 °C 4.3: 2 h / 25 - 90 °C 5.1: hydrogenchloride / methanol; water / 4 h / 30 - 70 °C View Scheme
反应条件
1.1: triethylsilane / dichloromethane / 20 - 25 °C 1.2: 3 h / -10 - 0 °C 1.3: 2.16 h / 25 °C 2.1: potassium carbonate / methanol / 28 °C 2.2: 2.4 h / 15 - 25 °C 2.3: 2 h / 25 - 90 °C 3.1: hydrogenchloride / methanol; water / 4 h / 30 - 70 °C View Scheme
反应条件
1.1: AlCl3, aluminium chloride / dichloromethane / 0.67 h / 0 °C 1.2: 5.5 h / -10 °C 2.1: triethylsilane / dichloromethane / 20 - 25 °C 2.2: 3 h / -10 - 0 °C 2.3: 2.16 h / 25 °C 3.1: potassium carbonate / methanol / 28 °C 3.2: 2.4 h / 15 - 25 °C 3.3: 2 h / 25 - 90 °C 4.1: hydrogenchloride / methanol; water / 4 h / 30 - 70 °C View Scheme
反应条件
1: N,N-dimethyl-formamide / Reflux 2: hydrazine hydrate / ethanol / 2 h / Reflux View Scheme
反应条件
1: N,N-dimethyl-formamide / 2 h / Reflux 2: hydrazine hydrate / ethanol / 2 h / Reflux View Scheme
反应条件
1: hydrogenchloride / ethyl acetate / 0.5 h / 0 - 5 °C 2: sulfur / 0.5 h / 180 - 185 °C View Scheme
反应条件
1.1: potassium carbonate / methanol / 30 °C 1.2: 1.67 h / 30 - 60 °C 2.1: sodium methylate / 4.5 h / 30 - 80 °C 2.2: 4.5 h / 80 - 100 °C 3.1: hydrogenchloride / methanol; water / 4 h / 30 - 70 °C View Scheme
反应条件
1.1: sodium methylate / 4.5 h / 30 - 80 °C 1.2: 4.5 h / 80 - 100 °C 2.1: hydrogenchloride / methanol; water / 4 h / 30 - 70 °C View Scheme
