γ-甲基-Alpha-三氟甲基-γ-丁内酯合成路线 (共 5 条)
反应条件
zinc(II) tetrahydroborate in diethyl ether T=20°C; 8 h;
参考文献
Palecek, Jiri; Kvicala, Jaroslav; Paleta, Oldrich
Journal of Fluorine Chemistry, 2002 , vol. 113, # 2 p. 177 - 183
反应条件
epoxysulfonyl fluoride in trifluoroacetic acid 2 h; Heating;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 40, # 12 p. 2447 - 2451
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 40, # 12 p. 2805 - 2809
反应条件
epoxysulfonyl fluoride in trifluoroacetic acid 2 h; Heating;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 40, # 12 p. 2447 - 2451
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 40, # 12 p. 2805 - 2809
反应条件
1: 65 percent / K2CO3 / H2O / 4 h / 45 °C 2: FSO3H / trifluoroacetic acid / 2 h / Heating View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 40, # 12 p. 2447 - 2451
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 40, # 12 p. 2805 - 2809
参考文献
Reineke, Ninja; Zaidi, Naveed A.; Mitra, Manju; O'Hagan, David; Batsanov, Andrei S.; Howard, Judith A. K.; Naumov, Dmitri Y.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 2 p. 147 - 150