2-甲氧基-6-甲基苯甲酰胺合成路线 （共 7 条）
参考文献
Fisher, Lawrence E.; Muchowski, Joseph M.; Clark, Robin D.
Journal of Organic Chemistry, 1992 , vol. 57, # 9 p. 2700 - 2705
反应条件
1: 91 percent / LDA / tetrahydrofuran; hexane / -70 deg C, 10 min, then to 0 deg C 2: 1.) tert-butyllithium / 1.) THF, pentane, -100 deg C, 10 min , then to -70 deg C 2.) THF, to 0 deg C 3: 86 percent / 50 percent aq. acetic acid / 60 °C View Scheme
参考文献
Fisher, Lawrence E.; Muchowski, Joseph M.; Clark, Robin D.
Journal of Organic Chemistry, 1992 , vol. 57, # 9 p. 2700 - 2705
反应条件
1: 1.) tert-butyllithium / 1.) THF, pentane, -100 deg C, 10 min , then to -70 deg C 2.) THF, to 0 deg C 2: 86 percent / 50 percent aq. acetic acid / 60 °C View Scheme
参考文献
Fisher, Lawrence E.; Muchowski, Joseph M.; Clark, Robin D.
Journal of Organic Chemistry, 1992 , vol. 57, # 9 p. 2700 - 2705
参考文献
Gibson
Journal of the Chemical Society, 1923 , vol. 123, p. 1272
反应条件
pyridine; trifluoroacetic anhydride in dichloromethane Ambient temperature;
参考文献
Fisher, Lawrence E.; Muchowski, Joseph M.; Clark, Robin D.
Journal of Organic Chemistry, 1992 , vol. 57, # 9 p. 2700 - 2705
反应条件
nitrosyl-sulphuric acid; water in dichloromethane Ambient temperature;
参考文献
Fisher, Lawrence E.; Muchowski, Joseph M.; Clark, Robin D.
Journal of Organic Chemistry, 1992 , vol. 57, # 9 p. 2700 - 2705
反应条件
1: nitrous acid 2: permanganate; natrium carbonate View Scheme
参考文献
Corbellini; Ravazzoni
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1931 , vol. <6> 13, p. 132,135
Full Text Show Details
Gibson
Journal of the Chemical Society, 1923 , vol. 123, p. 1272
