3-叠氮基-3-脱氧-1,2:5,6-二-o-异亚丙基-alpha-d-呋喃葡萄糖合成路线 （共 14 条）
反应条件
lithium azide in N,N-dimethyl-formamide T=25°C; 24 h;
参考文献
Sleath, Paul R.; Handlon, Anthony L.; Oppenheimer, Norman J.
Journal of Organic Chemistry, 1991 , vol. 56, # 11 p. 3608 - 3613
反应条件
sodium azide in N,N-dimethyl-formamide T=130°C; 10 h;
参考文献
US2008/114031 A1, ;
Page/Page column 18 ;
反应条件
1: With pyridine; trifluoromethylsulfonic anhydride in dichloromethane T=-20°C; 2: With sodium azide in N,N-dimethyl-formamide T=50°C; Further stages.;
参考文献
Danac, Ramona; Ball, Lucy; Gurr, Sarah J.; Fairbanks, Antony J.
Carbohydrate Research, 2008 , vol. 343, # 6 p. 1012 - 1022
反应条件
sodium azide in N,N-dimethyl-formamide T=110°C; 48 h;
参考文献
Gurjar, M. K.; Patil, V. J.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 1017 - 1020
反应条件
1: 90 percent / NaBH4 / ethanol; H2O / 1 h / 0 °C 2: pyridine / CH2Cl2 / 0.75 h / -30 °C 3: 14.1 g / NaN3 / dimethylformamide / 50 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 124, # 36 p. 10642 - 10643
反应条件
1: 91 percent / pyridinium dichromate; acetic anhydride / CH2Cl2 / 4 h / 75 °C 2: 90 percent / NaBH4 / ethanol; H2O / 1 h / 0 °C 3: pyridine / CH2Cl2 / 0.75 h / -30 °C 4: 14.1 g / NaN3 / dimethylformamide / 50 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 124, # 36 p. 10642 - 10643
反应条件
1: 68 percent / ZnCl2; aq. H3PO4 / 36 h / 20 °C 2: 91 percent / pyridinium dichromate; acetic anhydride / CH2Cl2 / 4 h / 75 °C 3: 90 percent / NaBH4 / ethanol; H2O / 1 h / 0 °C 4: pyridine / CH2Cl2 / 0.75 h / -30 °C 5: 14.1 g / NaN3 / dimethylformamide / 50 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 124, # 36 p. 10642 - 10643
反应条件
1: pyridine 2: NaN3, 15-crown-5 View Scheme
参考文献
Journal of the American Chemical Society, , vol. 120, # 38 p. 9951 - 9952
反应条件
sodium azide in 2-methoxy-ethanol Substitution; azidation; 7 h; Heating;
参考文献
Yoshimura, Yuichi; Endo, Mikari; Miura, Shinji; Sakata, Shinji
Journal of Organic Chemistry, 1999 , vol. 64, # 21 p. 7912 - 7920
反应条件
in toluene T=60°C; 1 h; Yield given;
参考文献
Liebigs Annalen der Chemie, , # 7 p. 1245 - 1260
