5-甲氧基-1-[(4-甲基苯基)磺酰基]-1H-吲哚合成路线 （共 7 条）
反应条件
1: With tris-trimethylsilyloxyethylene; Grubb's 2nd generation catalyst in dichloromethane 1.5 h; Heating; 2: With Grubb's 2nd generation catalyst in benzene 3 h; Heating;
参考文献
Arisawa, Mitsuhiro; Terada, Yukiyoshi; Takahashi, Kazuyuki; Nakagawa, Masako; Nishida, Atsushi
Journal of Organic Chemistry, 2006 , vol. 71, # 11 p. 4255 - 4261
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane T=20°C; Cyclization; 3 h;
参考文献
Tohma, Hirofumi; Watanabe, Hiroaki; Takizawa, Shinobu; Maegawa, Tomohiro; Kita, Yasuyuki
Heterocycles, 1999 , vol. 51, # 8 p. 1785 - 1788
反应条件
propionic acid in propionic acid 46 h; Heating;
参考文献
Murai, Yasushi; Kobayashi, Shougo; Inoue, Seiichi; Sato, Kikumasa
Heterocycles, 1992 , vol. 34, # 5 p. 1017 - 1029
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in toluene 2 h; Ambient temperature;
参考文献
Zheng, Qi; Yang, Youhua; Martin, Arnold R.
Heterocycles, 1994 , vol. 37, # 3 p. 1761 - 1772
反应条件
1: 1.) N-chlorosuccinimide, 2.) triethylamine / 1.) CH2Cl2, -30 deg C, 30 min, 2.) CH2Cl2, reflux, 2 h 2: 94 percent / CH2Cl2 / 2 h / Ambient temperature 3: 92 percent / propionic acid / propionic acid / 46 h / Heating View Scheme
参考文献
Murai, Yasushi; Kobayashi, Shougo; Inoue, Seiichi; Sato, Kikumasa
Heterocycles, 1992 , vol. 34, # 5 p. 1017 - 1029
反应条件
1: 94 percent / CH2Cl2 / 2 h / Ambient temperature 2: 92 percent / propionic acid / propionic acid / 46 h / Heating View Scheme
参考文献
Murai, Yasushi; Kobayashi, Shougo; Inoue, Seiichi; Sato, Kikumasa
Heterocycles, 1992 , vol. 34, # 5 p. 1017 - 1029
反应条件
caesium carbonate in tetrahydrofuran; methanol T=64°C; 2.5 h;
参考文献
Liu, Yugang; Shen, Lichun; Prashad, Mahavir; Tibbatts, Jessica; Repic, Oljan; Blacklock, Thomas J.
Organic Process Research and Development, 2008 , vol. 12, # 4 p. 778 - 780
