1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / 0 - 20 °C / |Inert atmosphere 2: hydrogen bromide / 5 h / 150 °C View Scheme

lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C; 5 h; Inert atmosphere;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '21729736', constants.ctx, '0')">palladium 10 on activated carbon</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '3587189', constants.ctx, '0')">hydrogen</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1098229', constants.ctx, '0')">methanol</a> <br />T=20&deg;C;&nbsp;2&nbsp;h;&nbsp;<br /> <br /> &nbsp;

<b>Multi-step reaction with 3 steps<br /> </b>1: triethylamine / 12 h / 60 &deg;C / |Inert atmosphere<br />2: CaO; phosphorous pentoxide / chloroform / |Inert atmosphere<br />3: triethylamine / acetonitrile / 1 h / 150 &deg;C / |Inert atmosphere; |Sealed tube; |Microwave irradiation<br /> <br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '605283', constants.ctx, '0')">triethylamine</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '741857', constants.ctx, '0')">acetonitrile</a> <br />T=150&deg;C;&nbsp;Diels-Alder Cycloaddition;&nbsp;1&nbsp;h;&nbsp;&nbsp;Inert atmosphereSealed tubeMicrowave irradiation;&nbsp;<br /> &nbsp;