反应条件
1.1: potassium carbonate; dimethyloctadecylbenzylammonium chloride; nitromethane / N,N-dimethyl-formamide / 48 h / 90 °C 2.1: acetic acid / N,N-dimethyl-formamide / 0.5 h / 45 °C 2.2: 4 h 3.1: potassium carbonate / 0 - 20 °C 4.1: triethylamine / dichloromethane / 0 °C 5.1: potassium formiate; formic acid / acetic anhydride / 100 °C View Scheme
参考文献
Zhang, Bin; Chen, Hongli; Tang, Huanyu; Feng, Huijin; Li, Yuanchao
Steroids, 2012 , vol. 77, # 11 p. 1086 - 1091