反应条件
<b>Multi-step reaction with 3 steps<br /> </b>1: 1.) NaH / 1.) benzene, reflux, 14 h, 2.) benzene, reflux, 4 d<br />2: 40 percent / LiAlH<sub>4</sub> / toluene; diethyl ether / 0.5 h<br />3: 65 percent / Et<sub>3</sub>N / CH<sub>2</sub>Cl<sub>2</sub> / 0.5 h / 0 °C<br /> <br />
参考文献
Stein, Thomas M.; Gellman, Samuel H. Journal of the American Chemical Society, 1992 , vol. 114, # 10 p. 3943 - 3950
