1-叠氮-1-脱氧-β-D-吡喃葡萄糖苷四乙酸酯合成路线 （共 38 条）
反应条件
trimethylsilylazide; tin(IV) chloride in dichloromethane T=20°C; 24 h;
参考文献
Bianchi, Aldo; Bernardi, Anna
Journal of Organic Chemistry, 2006 , vol. 71, # 12 p. 4565 - 4577
反应条件
sodium azide in dimethyl sulfoxide T=20°C; 0.333333 h;
参考文献
Jha, Abadh Kishor; Jain, Nidhi
Tetrahedron Letters, 2013 , vol. 54, # 35 p. 4738 - 4741
反应条件
trimethylsilylazide; tin(IV) chloride in dichloromethane T=20°C; stereoselective reaction;
参考文献
Carroux, Cindy J.; Moeker, Janina; Motte, Josephine; Lopez, Marie; Bornaghi, Laurent F.; Katneni, Kasiram; Ryan, Eileen; Morizzi, Julia; Shackleford, David M.; Charman, Susan A.; Poulsen, Sally-Ann
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 2 p. 455 - 459
反应条件
trimethylsilylazide; tetra-n-butylammonium difluorotriphenylsilicate(IV) in tetrahydrofuran T=65°C; Substitution; 20 h;
参考文献
Soli, Eric D.; DeShong, Philip
Journal of Organic Chemistry, 1999 , vol. 64, # 26 p. 9724 - 9726
反应条件
sodium azide; tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate in dichloromethane; water T=20°C; 3 h;
参考文献
Sirion, Uthaiwan; Kim, Hee Jun; Lee, Jae Hak; Seo, Jai Woong; Lee, Byoung Se; Lee, Sang Ju; Oh, Seung Jun; Chi, Dae Yoon
Tetrahedron Letters, 2007 , vol. 48, # 23 p. 3953 - 3957
反应条件
trimethylsilylazide; tin(IV) chloride in dichloromethane T=20°C; 2 h;
参考文献
Cagnoni, Alejandro J.; Varela, Oscar; Gouin, Sebastien G.; Kovensky, Jose; Uhrig, Maria Laura
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3064 - 3077
反应条件
1: With hydrogen bromide in acetic acid T=0 - 20°C; 2: With hydrogen bromide in acetic acid T=0 - 20°C; 3: With sodium azide; tetra(n-butyl)ammonium hydrogensulfate; sodium carbonate in dichloromethane T=20°C; 1.5 h;
参考文献
Kumar, Rishi; Tiwari, Pallavi; Maulik, Prakas R.; Misra, Anup K.
European Journal of Organic Chemistry, 2006 , # 1 p. 74 - 79
反应条件
1: With hydrogen bromide in dichloromethane; acetic acid T=0°C; Inert atmosphere; 2: With sodium azide in N,N-dimethyl-formamide T=20°C; 3 h; Inert atmosphere;
参考文献
European Journal of Medicinal Chemistry, , vol. 63, p. 782 - 792
参考文献
Mugunthan; Kartha, K.P. Ravindranathan
Journal of Carbohydrate Chemistry, 2008 , vol. 27, # 5 p. 294 - 299
反应条件
in N,N-dimethyl-formamide
参考文献
Eisai Co., Ltd.
Patent: US5986088 A1, 1999 ;
