1-叠氮-1-脱氧-β-D-吡喃葡萄糖苷四乙酸酯合成路线 （共 38 条）
反应条件
1: pyridine / 16 h / 20 °C 2: hydrogen bromide; acetic acid / 1 h / 0 - 20 °C 3: sodium azide / N,N-dimethyl-formamide / 0.17 h / 80 °C / |Microwave irradiation; |Sealed tube View Scheme
参考文献
Asian Journal of Chemistry, , vol. 24, # 12 p. 5592 - 5596,5
Asian Journal of Chemistry, , vol. 24, # 12 p. 5592 - 5596
反应条件
pyridine; sodium azide 1) 2-methoxyethanol, 100 deg C, overnight, 2) 2 h; Yield given. Multistep reaction;
参考文献
Carbohydrate Research, , vol. 210, p. 333 - 337
反应条件
1: diethyl ether; silver azide 2: pyridine View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 592, p. 54,65
参考文献
Justus Liebigs Annalen der Chemie, , vol. 592, p. 54,65
反应条件
sodium azide 1.) DMF, 70 deg C, 6 h, 2.) pyridine, 20 deg C; Yield given. Multistep reaction;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 30, # 7 p. 1329 - 1331
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 7 p. 1638 - 1641
反应条件
hydrogen; palladium on activated charcoal
参考文献
Van Ameijde, Jeroen; Albada, H. Bauke; Liskamp, Rob M.J.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 8 p. 1042 - 1049
反应条件
tin(IV) chloride in dichloromethane; N,N-dimethyl-formamide T=20°C; 24 h; Solvent;
参考文献
Sahoo, Laxminarayan; Singhamahapatra, Anadi; Paul, Katuri J.V.; Loganathan, Duraikkannu
Tetrahedron Letters, 2013 , vol. 54, # 39 p. 5361 - 5365
反应条件
tin(IV) chloride in dichloromethane; N,N-dimethyl-formamide T=20°C; 24 h; Solvent;
参考文献
Sahoo, Laxminarayan; Singhamahapatra, Anadi; Paul, Katuri J.V.; Loganathan, Duraikkannu
Tetrahedron Letters, 2013 , vol. 54, # 39 p. 5361 - 5365
参考文献
Neto, Virginie; Granet, Robert; Mackenzie, Grahame; Krausz, Pierre
Journal of Carbohydrate Chemistry, 2008 , vol. 27, # 4 p. 231 - 237
参考文献
Bovin, N. V.; Zurabyan, S. E.; Khorlin, A. Ya.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 7 p. 1329 - 1331
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 7 p. 1638 - 1641
