反应条件
n-butyllithium in tetrahydrofuran; hexane byproducts: LiCl; addn. of n-BuLi in hexane to dry NH3 in abs. THF at -30°C (inert gas), addn. of the Ge compd. in THF at room temp.; stored at 20°C for 48 h; evapn., addn. of benzene, filtn. (LiCl) and evapn.;
参考文献
Riviere-Baudet, Monique; Morere, Alain; Onyszchuk, Mario; Satge, Jacques
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 70, # 1/2 p. 75 - 90
