反应条件
1: 95 percent / 40 aq. percent NaOH, trimethylbenzylammonium chloride / benzene / 17 h / Heating 2: 75 percent / H2 / 10 percent Pd-C / ethanol 3: 72 percent / triethylamine / benzene / 3 h 4: NaOEt / ethanol / 20 h / Heating 5: H2O; acetonitrile / 2 h / Heating 6: 66 percent / triethylamine, toluene-p-sulphonyl azide / acetonitrile / 1.) 0 deg C, 1 h, 2.) RT, 2 h 7: 50 percent / H2O / diethyl ether / 0.75 h / Irradiation 8: 80 percent / toluene / 2 h / Heating 9: 85 percent / diborane-THF complex / 2 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 877 - 884
