反应条件
1: H2O; acetonitrile / 2 h / Heating 2: 66 percent / triethylamine, toluene-p-sulphonyl azide / acetonitrile / 1.) 0 deg C, 1 h, 2.) RT, 2 h 3: 50 percent / H2O / diethyl ether / 0.75 h / Irradiation 4: 80 percent / toluene / 2 h / Heating 5: 85 percent / diborane-THF complex / 2 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 877 - 884