1: With titanium(IV) isopropylate in tetrahydrofuran; diethyl ether T=20°C; 1 h; 2: With boron trifluoride diethyl etherate in tetrahydrofuran; diethyl ether 1 h; 3: With sodium hydroxide; water in tetrahydrofuran; diethyl ether
参考文献
ABBOTT GMBH and CO. KG
Patent: WO2006/40179 A1, 2006 ;
Location in patent: Page/Page column 97 ;
WO 2006/040179 A1
1: With titanium(IV) isopropylate in tetrahydrofuran T=20°C; 1 h; 2: With boron trifluoride diethyl etherate in diethyl ether T=20°C; 0.5 h; 3: With sodium hydroxide Further stages.;
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3 platinum on carbon; hydrogen in toluene T=105°C; P=4500.45 Torr; Flow reactor;
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Lieber et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 654,655
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