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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
乙酸对甲酚酯
合成路线
（共 120 条）
140-39-6
乙酸对甲酚酯
→
反应条件
88952-72-1
反应条件
1: AlCl3 2: 91 percent / pyridine / 0.5 h / 50 °C 3: 85 percent / pyridine; KOH / 1.5 h / 50 °C 4: 85 percent / conc. H2SO4 / acetic acid / 2 h / 80 °C View Scheme
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
140-39-6
乙酸对甲酚酯
→
反应条件
88952-74-3
反应条件
1: AlCl3 2: 82 percent / pyridine / 0.5 h / 50 °C 3: 96 percent / pyridine; KOH / 1.5 h / 50 °C 4: 91 percent / conc. H2SO4 / acetic acid / 2 h / 80 °C View Scheme
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
140-39-6
乙酸对甲酚酯
→
反应条件
71-50-1
冰醋酸
+
22113-51-5
反应条件
borate buffer; THEA16Cl in water T=20°C; various quaternary ammonium salts, hydrolysis; Rate constant;
参考文献
Kulic, Jiri; Sussenbek, Jiri; Ptacek, Ales
Collection of Czechoslovak Chemical Communications, 1993 , vol. 58, # 12 p. 2891 - 2895
140-39-6
乙酸对甲酚酯
→
反应条件
89112-85-6
反应条件
1: AlCl3 2: 87 percent / pyridine / 0.5 h / 50 °C 3: 76 percent / pyridine; KOH / 1.5 h / 50 °C 4: 96 percent / conc. H2SO4 / acetic acid / 2 h / 80 °C View Scheme
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
140-39-6
乙酸对甲酚酯
→
反应条件
89112-88-9
反应条件
1: AlCl3, aluminium chloride / 2 h / 120 - 180 °C 2: potassium carbonate / acetone / 12 h / |Reflux 3: sodium acetate; acetic acid / 12 h / |Reflux View Scheme
参考文献
Wang, Xiao-Bing; Yang, Lei; Kong, Ling-Yi; Liu, Wei; Guo, Qing-Long
Medicinal Chemistry Research, 2012 , vol. 21, # 8 p. 1833 - 1849,17
140-39-6
乙酸对甲酚酯
→
反应条件
468060-75-5
反应条件
1: AlCl3 2: 91 percent / pyridine / 0.5 h / 50 °C 3: 85 percent / pyridine; KOH / 1.5 h / 50 °C 4: 85 percent / conc. H2SO4 / acetic acid / 2 h / 80 °C 5: 92 percent / BBr3 / CH2Cl2 / 18 h / -78 - 20 °C View Scheme
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
140-39-6
乙酸对甲酚酯
→
反应条件
50400-51-6
反应条件
1: AlCl3, aluminium chloride / 2 h / 120 - 180 °C 2: potassium carbonate / acetone / 12 h / |Reflux 3: sodium acetate; acetic acid / 12 h / |Reflux 4: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 12 h / |Reflux View Scheme
参考文献
Wang, Xiao-Bing; Yang, Lei; Kong, Ling-Yi; Liu, Wei; Guo, Qing-Long
Medicinal Chemistry Research, 2012 , vol. 21, # 8 p. 1833 - 1849,17
140-39-6
乙酸对甲酚酯
→
反应条件
56609-15-5
反应条件
1: hydrogenchloride / AlCl3 2: bromine; iron / dichloromethane; water View Scheme
参考文献
Giesbrecht, Garth R.; Boller, Timothy M.; Voskoboynikov, Alexander Z.; Asachenko, Andrey F.; Nikulin, Mikhail V.; Tsarev, Alexey A.
Patent: US2011/98425 A1, 2011 ;
140-39-6
乙酸对甲酚酯
→
反应条件
57479-56-8
反应条件
1: 90 percent / AlCl3 2: 1.) NaH; 2.) LDA / 1.) THF; 2.) THF, -78 deg C, 15 min. 3: 90 percent / NaOMe / ethanol / 19 h / Heating 4: 1.) Et3N, CH3SO2Cl; 2.) LiAlH4 / 1.) THF, -23 deg C, 1 h; 2.) ether, room temp., 2 h 5: HBr / pentane / 0.17 h 6: TiCl4 / CH2Cl2 / 0.5 h, -20 deg C, 10 h, room temp. View Scheme
参考文献
Solladie, Guy; Girardin, Andre
Bulletin de la Societe Chimique de France, 1987 , # 1 p. 123 - 124
67-62-9
3-氯苯甲酰乙腈
+
140-39-6
乙酸对甲酚酯
→
反应条件
106-44-5
对甲酚
+
5806-90-6
N-甲氧基-乙酰胺
反应条件
acetate buffer in water T=25°C; other acidic catalysts with various pKa; effect of viscosity (aq. glycerol) on rate constants; MechanismRate constant;
参考文献
Cox, Michael M.; Jencks, William P.
Journal of the American Chemical Society, 1981 , vol. 103, # 3 p. 572 - 580
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