N,N'-二乙酰-1,4-苯二胺合成路线 （共 31 条）
反应条件
1: acetic acid; acetic acid anhydride; nitrogen oxides 3: HNO3; acetic acid anhydride / 0 °C / zuletzt bei 45-50grad View Scheme
参考文献
Journal of the Chemical Society, , p. 1364,1371
Journal of the Chemical Society, , p. 369,371
反应条件
chlorine in acetic acid; N,N-dimethyl-formamide T=45°C;
参考文献
Avdeenko; Marchenko
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 6 p. 822 - 829
反应条件
1: acetic acid; acetic acid anhydride; nitrogen oxides 3: bromine; iodine; glacial acetic acid View Scheme
参考文献
France; Heilbron; Hey
Journal of the Chemical Society, 1938 , p. 1364,1371
Journal of the Chemical Society, 1940 , p. 369,371
反应条件
1: acetic acid; acetic acid anhydride; nitrogen oxides 3: bromine; iodine; glacial acetic acid View Scheme
参考文献
France; Heilbron; Hey
Journal of the Chemical Society, 1938 , p. 1364,1371
Journal of the Chemical Society, 1940 , p. 369,371
反应条件
sulfuric acid; iron(II) sulfate; nitrobenzene
参考文献
Wiley et al.
Journal of Organic Chemistry, 1958 , vol. 23, p. 268,271
反应条件
trichlorophosphate T=75°C; 16 h;
参考文献
Meth-Cohn, Otto; Narine, Bramha; Tarnowski, Brian
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1520 - 1530
反应条件
1: 1.) NaH
2: aq. H2SO4 / Heating
3: NaNO2
View Scheme
参考文献
Namiki; Arai; Fujimori
Journal of the American Chemical Society, 1997 , vol. 119, # 16 p. 3840 - 3841
反应条件
1.1: 64.2 percent / H2SO4 / 3 h / 50 °C
2.1: H2SO4 / 5 h / 100 °C
2.2: 70 percent / aq. NH3
View Scheme
参考文献
Dzierzbicka, Krystyna; Trzonkowski, Piotr; Sewerynek, Przemyslaw; Mysliwski, Andrzej
Journal of Medicinal Chemistry, 2003 , vol. 46, # 6 p. 978 - 986
反应条件
nitrogen oxides; acetic anhydride; acetic acid
参考文献
France; Heilbron; Hey
Journal of the Chemical Society, 1940 , p. 369
Journal of the Chemical Society, 1939 , p. 1288,1291
反应条件
1: lead (IV)-acetate
2: acetic acid; water; HCl
View Scheme
参考文献
Adams; Anderson
Journal of the American Chemical Society, 1950 , vol. 72, p. 5154,5157
