2-甲基-5-乙烯基吡啶合成路线 （共 24 条）
反应条件
potassium hydroxide; water; dimethyl sulfoxide; hydroquinone
T=70°C; 4 h; Yield given. Yields of byproduct given;
参考文献
Gusarova; Malysheva; Belogorlova; Arbuzova; Gendin; Trofimov
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 8 p. 1156 - 1159
反应条件
potassium phosphate in isobutyramide
T=100°C; 22 h;
参考文献
MEDIVATION NEUROLOGY, INC.
Patent: WO2009/111540 A1, 2009 ;
Location in patent: Page/Page column 29-30 ;
反应条件
phosphoric acid in methanol; water
T=-5 - 25°C; 4 h;
参考文献
LONZA LTD; BRENNER, Meinrad; ELZNER, Stephan; MILLER, Raimund
Patent: WO2011/150950 A1, 2011 ;
Location in patent: Page/Page column 6 ;
反应条件
sodium hydroxide; dimethylsulfide borane complex; dihydrogen peroxide
1.) THF, 65 deg C, 9 h; other vinyl and propenyl heterocycles; other pyridine-BF3 complexes; other hydroborating agents; var. temp. and time; Product distribution;
参考文献
Brown, Herbert C.; Prasad, J. V. N. Vara; Zee, Sheng-Hsu
Journal of Organic Chemistry, 1986 , vol. 51, # 4 p. 439 - 445
