二硫代甲酸-O-1-甲基乙酯钾盐合成路线 (共 39 条)
反应条件
in N,N-dimethyl-formamide 0.0666667 h; Microwave irradiation; TemperatureTime;
参考文献
Mahesh Kumar; Dubey
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2012 , vol. 51, # 11 p. 1619 - 1622
反应条件
hydrogenchloride in water T=35.1°C; ΔH(excit.), ΔS(excit.), ΔF(excit.); further temperature; further acid concentrations; KineticsMechanismThermodynamic data;
参考文献
Pandian, Daisy G.; Gnanadoss, Lalitha; Madhurambal, G.
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical & Analytical, 1982 , vol. 21, # 5 p. 511 - 513
反应条件
in N,N-dimethyl-formamide
0.0833333 h; Microwave irradiation; TemperatureTime;
参考文献
Mahesh Kumar; Dubey
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2012 , vol. 51, # 11 p. 1619 - 1622
反应条件
1: in acetone
Substitution; 3 h; Heating;
2: With sulfuric acid in acetone
T=0°C; Cyclization; 2 h;
参考文献
Sakurai, Naoki; Mori, Hatsumi; Tanaka, Shoji; Moriyama, Hiroshi
Chemistry Letters, 1999 , # 11 p. 1191 - 1192
反应条件
disulfur dichloride in diethyl ether
T=25°C; 1 h;
参考文献
Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 1986 , vol. 51, # 10 p. 1866 - 1881
反应条件
in isopropyl alcohol
T=70 - 75°C; 4 h;
参考文献
Mustafaev; Kulieva; Kulibekova; Kakhramanova; Safarova; Novotorzhina
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 2 p. 198 - 203
Zh. Org. Khim., 2013 , vol. 49, # 2 p. 210 - 214,5
反应条件
1:
2: With perchloric acid
参考文献
Pintus, Anna; Aragoni, M. Carla; Bellec, Nathalie; Devillanova, Francesco A.; Lorcy, Dominique; Isaia, Francesco; Lippolis, Vito; Randall, Rebecca A. M.; Roisnel, Thierry; Slawin, Alexandra M. Z.; Woollins, J. Derek; Arca, Massimiliano
European Journal of Inorganic Chemistry, 2012 , # 22 p. 3577 - 3594
反应条件
1: in acetone
1 h; Reflux;
2: With perchloric acid in chloroform
6 h; Reflux;
参考文献
Qu, Li; Guo, Yunlong; Luo, Hao; Zhong, Cheng; Yu, Gui; Liu, Yunqi; Qin, Jingui
Chemical Communications, 2012 , vol. 48, # 80 p. 9965 - 9967
参考文献
Bhattacharya,A.K.; Hortmann,A.G.
Journal of Organic Chemistry, 1974 , vol. 39, p. 95 - 99
参考文献
Inoue, Jun-Ichi; Kanno, Masato; Ashizawa, Minoru; Seo, Chayeon; Tanioka, Akihiko; Mori, Takehiko
Chemistry Letters, 2010 , vol. 39, # 6 p. 538 - 540