二硫代甲酸-O-1-甲基乙酯钾盐合成路线 (共 39 条)
参考文献
Ambrosio, Lucia; Aragoni, M. Carla; Arca, Massimiliano; Devillanova, Francesco A.; Hursthouse, Michael B.; Huth, Susanne L.; Isaia, Francesco; Lippolis, Vito; Mancini, Annalisa; Pintus, Anna
Chemistry - An Asian Journal, 2010 , vol. 5, # 6 p. 1395 - 1406
参考文献
Bhattacharya,A.K.; Hortmann,A.G.
Journal of Organic Chemistry, 1974 , vol. 39, p. 95 - 99
参考文献
Bhattacharya,A.K.; Hortmann,A.G.
Journal of Organic Chemistry, 1974 , vol. 39, p. 95 - 99
参考文献
Bhattacharya,A.K.; Hortmann,A.G.
Journal of Organic Chemistry, 1974 , vol. 39, p. 95 - 99
参考文献
Bhattacharya,A.K.; Hortmann,A.G.
Journal of Organic Chemistry, 1974 , vol. 39, p. 95 - 99
反应条件
1: butanone With Me3SiCH2Br; dimethyl sulfoxide in acetonitrile
1 h; Inert atmosphereCooling with ice;
2: potassium isopropyl xanthate in acetonitrile
T=20°C; 1 h;
3: With perchloric acid in diethyl ether; chloroform; water
1 h; Reflux;
参考文献
The University of Tokyo
Patent: EP2256111 A1, 2010 ;
Location in patent: Page/Page column 13 ;
参考文献
Yamada, Jun-Ichi; Satoki, Shyuji; Mishima, Sachinori; Akashi, Nobutaka; Takahashi, Kouhei; Masuda, Nobuyuki; Nishimoto, Yasushi; Takasaki, Satoshi; Anzai, Hiroyuki
Journal of Organic Chemistry, 1996 , vol. 61, # 12 p. 3987 - 3995
参考文献
Schumaker,R.R.; Engler,E.M.
Journal of the American Chemical Society, 1977 , vol. 99, p. 5521 - 5522
反应条件
SCl2 in diethyl ether
T=25°C; 1 h;
参考文献
Schroll, Alayne L.; Barany, George
Journal of Organic Chemistry, 1986 , vol. 51, # 10 p. 1866 - 1881