2-甲硫基-4,6-二甲基嘧啶合成路线 （共 14 条）
反应条件
sodium hydroxide in water T=20°C; 1.16667 h;
参考文献
Abbott GmbH and Co., KG
Patent: US6670367 B1, 2003 ;
Location in patent: Page column 15 ;
反应条件
potassium carbonate in water T=25°C; Reflux;
参考文献
Lee, Yun Suk; Kim, Hye Yun; Kim, Youngsoo; Seo, Jae Hong; Roh, Eun Joo; Han, Hogyu; Shin, Kye Jung
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 16 p. 4921 - 4935
反应条件
sodium hydroxide 7 h; Ambient temperature;
参考文献
Ishizumi; Kojima; Antoku
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 9 p. 2288 - 2300
反应条件
tetrabutylammomium bromide; potassium carbonate T=90°C; P=760.051 Torr; 1 h;
参考文献
Xie, Jian-Gang; Quan, Jing; Li, Shu-Bai; Zheng, Yan; Zhu, Li-Min
Synthetic Communications, 2011 , vol. 41, # 6 p. 871 - 878
反应条件
1: 80 percent / HCl / ethanol / 2 h / Heating 2: 60 percent / aq. KOH View Scheme
参考文献
Bollettino chimico farmaceutico, , vol. 143, # 7 p. 275 - 279
反应条件
potassium carbonate 0.2 h; Microwave irradiation;
参考文献
Goswami, Shyamaprosad; Hazra, Anita; Jana, Subrata
Bulletin of the Chemical Society of Japan, 2009 , vol. 82, # 9 p. 1175 - 1181
反应条件
potassium carbonate in water; acetone 20 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 46, # 6 p. 911 - 916
参考文献
Journal of the American Chemical Society, , vol. 37, p. 598
反应条件
water; chlorine in dichloromethane T=0°C;
参考文献
Abbott GmbH and Co., KG
Patent: US6670367 B1, 2003 ;
Location in patent: Page column 15-16 ;
反应条件
1: 34.9 percent / 30percent aq. H2O2, HCOOH / 3 h / Ambient temperature 2: 65 percent / ethanol / 1.) ice bath, 2.) room temperature View Scheme
参考文献
Ishizumi; Kojima; Antoku
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 9 p. 2288 - 2300
