7-甲氧基-8-甲基-2H-色烯-2-酮合成路线 （共 8 条）
反应条件
1: 7-hydroxy-8-methyl-2H-chromen-2-one With sodium hydride in N,N-dimethyl-formamide T=0°C; 0.333333 h; 2: methyl iodide With sodium hydride in N,N-dimethyl-formamide T=0 - 20°C; 5 h;
参考文献
Leonetti, Francesco; Favia, Angelo; Rao, Angela; Aliano, Rosaria; Paluszcak, Anja; Hartmann, Rolf W.; Carotti, Angelo
Journal of Medicinal Chemistry, 2004 , vol. 47, # 27 p. 6792 - 6803
反应条件
ytterbium(III) triflate in nitromethane T=100°C; 1.5 h;
参考文献
Fillion, Eric; Dumas, Aaron M.; Kuropatwa, Bryan A.; Malhotra, Neil R.; Sitler, Tamsyn C.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 409 - 412
反应条件
1.1: 120 °C 1.2: 95 percent / H2SO4; CF3COOH / 0.5 h / 20 °C 2.1: NaH / dimethylformamide / 0.33 h / 0 °C 2.2: 36 percent / NaH / dimethylformamide / 5 h / 0 - 20 °C View Scheme
参考文献
Seshadri; Venkateswarlu
Proceedings - Indian Academy of Sciences, Section A, 1941 , # 14 p. 297,304
反应条件
boron trifluoride in diethyl ether 0.025 h; microwave irradiation;
参考文献
Saidi, Mohammad R.; Rajabi, Fatemeh
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 11 p. 2343 - 2348
反应条件
1: palladium/charcoal; acetic acid / Hydrogenation 2: acetone; potassium carbonate View Scheme
参考文献
Seshadri; Venkateswarlu
Proceedings - Indian Academy of Sciences, Section A, 1941 , # 14 p. 297,304
反应条件
1: piperidine 2: ethanolic KOH-solution 3: quinoline; copper / 160 °C View Scheme
参考文献
Seshadri; Venkateswarlu
Proceedings - Indian Academy of Sciences, Section A, 1941 , # 14 p. 297,304
反应条件
1: ethanolic KOH-solution 2: quinoline; copper / 160 °C View Scheme
参考文献
Seshadri; Venkateswarlu
Proceedings - Indian Academy of Sciences, Section A, 1941 , # 14 p. 297,304
参考文献
Gupta; Seshadri
Journal of Scientific and Industrial Research, 1957 , vol. 16B, p. 257,260
Chem.Abstr., 1958 , p. 376
