1,5-二甲基-2-呋喃甲醇合成路线 (共 5 条)
反应条件
lithium in diethyl ether 0.166667 h; ultrasonic agitation;
参考文献
Luche, Jean-Louis; Damiano, Jean-Claude
Journal of the American Chemical Society, 1980 , vol. 102, # 27 p. 7926 - 7927
反应条件
in tetrahydrofuran T=-78°C;
参考文献
Marshall; Mapp; Heathcock
Journal of Organic Chemistry, 1996 , vol. 61, # 26 p. 9135 - 9145
反应条件
sodium tetrahydroborate in ethanol Inert atmosphere;
参考文献
Stepanenko, Viatcheslav; De Jesus, Melvin; Correa, Wildeliz; Bermudez, Lorianne; Vazquez, Cindybeth; Guzman, Irisbel; Ortiz-Marciales, Margarita
Tetrahedron Asymmetry, 2009 , vol. 20, # 23 p. 2659 - 2665
反应条件
n-butyllithium 1.) THF, RT, 4 h, 2.) THF, RT, 4 h; Yield given. Multistep reaction;
参考文献
Wu, Hsien-Jen; Lin, Shie-Hsiung; Lin, Chu-Chung
Heterocycles, 1994 , vol. 38, # 7 p. 1507 - 1518
反应条件
water; chlorine 1) methanol, room temp., 1.5 h, 2) 140 deg C; Yield given. Multistep reaction;
参考文献
Pfizer Inc.
Patent: US4082717 A1, 1978 ;