2,2-二甲基-1,3-苯并二恶茂烷合成路线 （共 36 条）
反应条件
1: acetic acid anhydride; chlorine 2: aqueous H2SO4 View Scheme
参考文献
Slooff
Recueil des Travaux Chimiques des Pays-Bas, 1935 , vol. 54, p. 995,999
反应条件
N-bromosuccinmide in N,N-dimethyl-formamide T=20°C; 48 h; Darkness;
参考文献
Sarker, Ashis K.; Kang, Man Gu; Hong, Jong-Dal
Dyes and Pigments, 2012 , vol. 92, # 3 p. 1160 - 1165
反应条件
N-bromosuccinmide in N,N-dimethyl-formamide
参考文献
Breslow, Ronald; Baugh, Simon D.P.
Patent: US2003/134824 A1, 2003 ;
反应条件
bromine; acetic anhydride
参考文献
Slooff
Recueil des Travaux Chimiques des Pays-Bas, 1935 , vol. 54, p. 995,999
反应条件
1: water; nitric acid
2: acetic acid; nitric acid
3: aqueous H2SO4
4: aqueous alkaline solution
View Scheme
参考文献
Slooff
Recueil des Travaux Chimiques des Pays-Bas, 1935 , vol. 54, p. 995,999
反应条件
sodium iodide in acetonitrile
10 h; Ambient temperature; Product distribution;
参考文献
Corda, Luciana; Fadda, Anna Maria; Maccioni, Antonio; Maccioni, Anna Maria; Podda, Gianni
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 311 - 314
反应条件
1: acetic acid anhydride; bromine
2: aqueous H2SO4
View Scheme
参考文献
Slooff
Recueil des Travaux Chimiques des Pays-Bas, 1935 , vol. 54, p. 995,999
反应条件
N-chloro-succinimide; n-butyllithium in tetrahydrofuran; hexane; dichloromethane; acetic acid
参考文献
E. I. Du Pont de Nemours and Company
Patent: US4502882 A1, 1985 ;
反应条件
boron trifluoride diethyl etherate in chloroform
T=20°C; 18 h;
参考文献
CORNELL UNIVERSITY; DICHTEL, William, R.; SPITLER, Eric, L.
Patent: WO2011/127301 A2, 2011 ;
Location in patent: Page/Page column 17 ;
反应条件
1: acetic acid anhydride; chlorine
2: water; nitric acid
View Scheme
参考文献
Slooff
Recueil des Travaux Chimiques des Pays-Bas, 1935 , vol. 54, p. 995,999
